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AL-LAD

  • Product Name: AL-LAD
  • CasNo: 65527-61-9
  • Purity:
  • Appearance: Pale Brown Solid

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CasNo： 65527-61-9

Molecular Formula： C22H27N3O

Appearance： Pale Brown Solid

Factory Supply industrial standard AL-LAD 65527-61-9 In Stock

  • Molecular Formula:C22H27N3O
  • Molecular Weight:349.476
  • Appearance/Colour:Pale Brown Solid 
  • Melting Point:>75°C (dec.) 
  • Boiling Point:558.2±50.0 °C(Predicted) 
  • PKA:17.31±0.40(Predicted) 
  • PSA：39.34000 
  • Density:1.18±0.1 g/cm3 (20 oC 760 Torr) 
  • LogP:3.40010 

65527-61-9 Relevant articles

Stereochemical and NMR Reassignment of 6-Norlysergic Acid Diethylamide and 6-Nor-6-allyllysergic Acid Diethylamide

Stachulski, Andrew V.,Nichols, David E.,Scheinmann, Feodor

, p. 30 - 31 (2007/10/03)

Conditions are described for the prepara...

Synthesis and LSD-like discriminative stimulus properties in a series of N(6)-alkyl norlysergic acid N,N-diethylamide derivatives

Hoffman,Nichols

, p. 1252 - 1255 (2007/10/02)

A convenient method for the synthesis of...

65527-61-9 Process route

allyl bromide
106-95-6

allyl bromide

8β-6-norlysergic acid diethylamide
35779-43-2

8β-6-norlysergic acid diethylamide

N-AllylnorLSD
65527-61-9

N-AllylnorLSD

Conditions
Conditions Yield
With potassium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 0.5h;
88%
9,10-didehydro-N,N-diethyl-6-cyanoergoline-8β-carboxamide
35779-41-0

9,10-didehydro-N,N-diethyl-6-cyanoergoline-8β-carboxamide

N-AllylnorLSD
65527-61-9

N-AllylnorLSD

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: 61 percent / Zn / acetic acid; H2O / 4 h / Heating
2: 88 percent / K2CO3 / dimethylformamide / 0.5 h / 25 °C
With potassium carbonate; zinc; In water; acetic acid; N,N-dimethyl-formamide;

65527-61-9 Upstream products

  • 106-95-6
    106-95-6

    allyl bromide

  • 35779-43-2
    35779-43-2

    8β-6-norlysergic acid diethylamide

  • 35779-43-2
    35779-43-2

    6-norlysergic acid diethylamide

  • 35779-41-0
    35779-41-0

    9,10-didehydro-N,N-diethyl-6-cyanoergoline-8β-carboxamide

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